| 引用本文: |
陈爱军,张喜利,张云莉,贺福元,刘珊,刘文龙,刘平安.葡萄糖原料碎米中12种有机磷农药残留快速检测[J].湖南中医药大学学报,2016,36(5):36-39[点击复制] |
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| 葡萄糖原料碎米中12种有机磷农药残留快速检测 |
| 陈爱军,张喜利,张云莉,贺福元,刘珊,刘文龙,刘平安 |
| (湖南环境生物职业技术学院, 湖南 衡阳 421005;湖南中医药大学中药超分子实验室, 湖南 长沙 410208;湖南安乡县北河口血防站, 湖南 常德 415600) |
| 摘要: |
| 目的 建立一种快速检测碎米中有机磷农药残留量的方法，用于注射用葡萄糖原料碎米的质量监控。方法 采用气相色谱法与氮磷检测器（NPD）快速检测碎米中的12种农药残留。结果 所建立的方法学的线性范围是0.1～5.0 ppm、检出限为0.98～6.24 ppb、检测限为3.27～20.8 ppb、相关系数均大于0.999 5；精密度、重复性的RSD均在6.3%以下；回收率在87.25%～108.4%。结论 本文建立了碎米中有机磷农药残留的快速检测方法，为注射用葡萄糖的制备筛选出合格的碎米原料提供了有效保障。 |
| 关键词: 碎米 注射用葡萄糖 气相色谱 有机磷农药残留 |
| DOI：10.3969/j.issn.1674-070X.2016.05.009 |
| 投稿时间：2015-09-28 |
| 基金项目:国家自然科学基金项目（30901971，81270055）；湖南省自然科学基金项目（14JJ2110，14JJ7061）。 |
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| Studies on the High-Speed Determination of the 12 Organophosphates Pesticides Residues in the Broken Rice for the Raw Material of Glucose Injection |
| CHEN Aijun,ZHANG Xili,ZHANG Yunli,HE Fuyuan,LIU Shan,LIU Wenlong,LIU Pingan |
| (Hunan Polytechnic of Environment and Biology, Hengyang, Hunan 421005, China;Laboratory of Supramolecular TCM, Hunan University of Chinese Medicine, Changsha, Hunan 410007, China;Hunan Schistosomiasis Control Station in Beihekou Anxiang, Changde, Hunan 415600, China) |
| Abstract: |
| objective To establish a determination method of the organophosphate in the broken rice, which can be used to control the glucose-injection quality. Methods 12 kinds of pesticides residues were rapid detected by using gas chromatography adding NDP detector. Results The linear range in the established determination method was 0.1~5.0 ppm, the limit of detection was 0.98~6.24 ppb, the limit of qualification was 3.27~20.8 ppb, and the correlation coefficient were all more than 0.995. Furthermore, the RSDs of the precision and repeatability tests were under 6.3%, the coeffecient of recovery was between 87.25%~108.4%. Conclusion This study had established a set of method to detect scientific organophosphorus pesticide residues. It will provide effective guarantee for screen raw broken-rice materials of the injection glucose. |
| Key words: broken rice injection glucose gas chromatography organophosphorus pesticide residues |
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