| 引用本文: |
王青 蔡
萍 万
丹 陈秋香.通宣益气丸的质量标准研究[J].湖南中医药大学学报,2011,31(7):29-31[点击复制] |
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| 通宣益气丸的质量标准研究 |
| 王青蔡
萍万
丹陈秋香 |
| (}1湖南中医药大学第二附属医院，湖南长沙410005;2湖南省中医药研究院，湖南长沙410006
3长沙市中医院，湖南长沙410010)) |
| 摘要: |
| 〔摘要〕目的建立通宣益气丸的质量标准〔方法采用薄层色谱法鉴别金银花、赤芍、黄茂，以高效液相色谱法
测定黄芬葺含量〔结果薄层鉴别中能检出金银花、赤芍、黄茂，阴性无干扰;HPLC测定黄芬葺在0.14-0.84 },g范围
内线性关系良好，r=0.9996，平均加样回收率为96.830Ic,RSD为1.68%结论木方法简便可行，可做为木品的质量控
制标准、 |
| 关键词: 通宣益气丸
薄层色谱法
高效液相色谱法
黄芩苷
质量标准 |
| DOI： |
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| 基金项目: |
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| Studyonquality standard of Tongxuan Yiqi pills |
| WANG Qing, CAI Ping, WAN Dan, CHEN Qiu-xiang |
| ((Second Affiliated Hospital, TCM University of Hunan, Changsha, Hunan, 410005, China) |
| Abstract: |
| [Abstract] Objective To
Set
up a quality standard of Tongxuan Yiqi pills. Methods The
TLC method
、、as
used for identifying Flos Lonicerae J
Astragals. The
Radix Paeoniae
content of Baicali was determined
aponicae, Radix Paeoniae Rubra and Radix
HPLC. Results Flos Lonicerae Japonicae,
Rubra and Radix Astragals could
detected with TLC without any
disturbing;
场I)e
the baicalin was
detected with HPLC
in a
good linear relation within the range of 0.140.84 N.,g,
r=0.999 6, the
average recovery rate was
96.83% and RSD
、、as
1.75%. Conclusion The method
is suitable for the aualitv control of Ton}xuan Yiai hills. |
| Key words: Tongxuan Yiqi pills TLC HPLC Baicali quality standard |
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