| 引用本文: |
李文亮 曾建国
刘发宝 张雪.一测多评法测定博落回果实中原阿片碱、
别隐品碱、血根碱和白屈菜红碱的含量[J].湖南中医药大学学报,2011,31(7):25-28[点击复制] |
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| 一测多评法测定博落回果实中原阿片碱、
别隐品碱、血根碱和白屈菜红碱的含量 |
| 李文亮曾建国
刘发宝张雪 |
| (}1湖南中医药大学，湖南长沙410208;2湖南农业大学，湖南长沙410007
3湖南省中药提取工程研究中心，湖南长沙410331)) |
| 摘要: |
| 〔摘要〕目的建立一测多评法测定博落回中原阿片碱、别隐品碱、血根碱和白屈菜红碱的含量〔方法以博落
回果实为研究对象，建立别隐品碱、血根碱、白屈菜红碱对原阿片碱的相对校正因子，利用该相对校正因子计算别
隐品碱、血根碱、白屈菜红碱的含量，实现一测多评;同时采用外标法测定药材中4种生物碱的含量，比较两种方法
的差异，验证一测多评法的准确性和可行性、结果9批博落回果实中4个生物碱的含量可以用一测多评法进行测
定，其计算值与实测值间无显著差异〔结论建立的一测多评法同步测定博落回果实中的原阿片碱、别隐品碱、血根
碱、白屈菜红碱是可行的、准确的、 |
| 关键词: 〔关键词〕博落回 生物碱 一测多评 相对校正因子 高效液相色谱法 |
| DOI： |
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| 基金项目:R284.2 |
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| Contents determination of protopine, allocryptopine,sanguinarine and chelerythrine in fruit of Macleaya cordatawith method of multi-assay depending on one determination |
| LI Wen-Bang, ZENG Jian-guo, LIU Fa-bao, ZHANG Xue |
| ((TCM University of Hunan, Changsha, Hunan, 410208, China)) |
| Abstract: |
| (Abstract〕 Objective To set up a method of multi-assay depending on one determination
[()detect the contents of umarine, allocryptopine, sanguinarine and chelerythrine in fruit of
Macleaya cordata (Willd.)R.Br. Methods The fruit of Macleaya cordata was studied[()set up the
relative correction factors of allocryptopine, sanguinarine and chelerythrine for detecting protopine,
and the factors were used[()measure the contents of allocryptopine, sanguinarine
and chelerythrine, and then, the method was set up. At the same time, other measurements used
[()detect the contents of the four alkaloids, comparing the two methods[()validate the accuracy
and feasibility of the new method. Results Four alkaloids contents in 9 batches of
Macleaya cordata were used the new method[()determine, and there were no signifi-
cant differences. Conclusion The new method is feasible and accurate[()evaluate the contents
of the four alkaloids in fructus of Macleaya cordata. |
| Key words: (Key words〕 Macleaya cordata R.Br.
(Willd.) alkaloids multi -assay depending
HPLC
()n
()ne
determination related correction factor(RCF) |
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